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| 內容簡介： |
《物理化学实验》（双语）为物理化学实验双语教材，内容涵盖绪论、实验技术、仪器操作、实验项目及附录。全书以简明实用为特色，系统介绍实验基础理论、测量方法及常用仪器使用规范，并精选九个经典实验，涵盖热力学、电化学、动力学与胶体化学等方向，注重培养学生综合应用能力。
本书可作为职业本科院校、高等职业院校、成人高校及本科院校的化工技术类及相关专业的实验教材，特别适合职教出海背景的高职本科类项目双语实验教学，也可供相关行业技术人员参考。
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| 目錄：
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第1章绪论
Chapter 1Introduction1
1.1物理化学实验目的和要求/1Purposes and requirements of physical chemistry experiments/2
1.2物理化学实验的安全防护/4Safety protection for physical chemistry experiments/6
1.3实验测量误差/11Experimental measurement error/12
1.4实验数据的表达与处理/15Expression and processing of experimental data/17
1.5物理化学实验中的计算机数据处理技术/19Computer data processing techniques in physical chemistry experiments/20
1.6实验考核要求/22Experimental evaluation requirements/23
第2章物理化学实验基本操作
Chapter 2Basic techniques of physical chemistry experiments26
2.1温度的测量/26Temperature measurement/31
2.2压力的测量/39Measurement of pressure/43
2.3流量的测量/48Flow measurement/50
第3章常用实验仪器使用方法
Chapter 3Usage of common experimental instruments53
3.1SYC-15E超级恒温槽/53SYC-15E super constant temperature bath/54
3.2FDY-Ⅱ双液系沸点测定仪/55FDY-Ⅱ dual liquid system boiling point tester/58
3.3WAY（2WAJ）阿贝折射仪/60WAY（2WAJ）Abbe refractometer/63
3.4DDS-11A型数字电导率仪/68DDS-11A digital conductivity meter/71
3.5UJ-25型电位差计/75UJ-25 potential difference meter/76
3.6电化学工作站/78Electrochemical workstation/80
3.7WZZ-2S自动旋光仪/83WZZ-2S automatic polarimeter/85
3.8DP-AW-Ⅰ表面张力实验装置/89DP-AW-Ⅰ surface tension experimental device/91
3.9DYY-2C型电泳仪/93DYY-2C electrophoresis meter/95
第4章实验项目
Chapter 4Experimental projects99
4.1恒温槽的安装与调试/99Installation and debugging of constant temperature bath/102
4.2液体饱和蒸气压的测定(动态法)/108Determination of saturated vapor pressure of liquid（dynamic method）/110
4.3双液系气-液平衡相图的绘制/114Drawing of vapor-liquid equilibrium phase diagrams for dual liquid systems/120
4.4乙酸电离常数的测定（电导法）/128Determination of ionization constant of acetic acid （conductometry）/132
4.5原电池电动势的测定/138Measurement of electromotive force of primary battery/142
4.6金属极化曲线的测定/148Determination of metal polarization curve/155
4.7蔗糖的转化——一级反应/166Conversion of sucrose——first order reaction/169
4.8溶液表面吸附量的测定/174Determination of surface adsorption capacity of solution/180
4.9胶体电泳/188Colloidal electrophoresis/191
附录
Appendix197
参考文献
References204
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为深入贯彻落实党的二十大对现代职业教育体系的战略部署，紧密围绕“职业教育定位为高技能人才培养、职业本科定位为高端技能人才培养”的新时代人才强国目标，本书面向职业本科院校与高等职业院校，结合“4+0”和“3+2”联合培养模式的教学实际，编写了这本注重实践性与前瞻性的物理化学实验教材，致力于为不同层次高素质技术技能人才的系统化培养提供专业支撑。
高等职业与本科联合培养项目是现代职教体系建设的重要突破，对提升高等职业院校教学质量与办学层次具有深远影响。该项目通过推动课程设置、教学内容及评价标准与本科教育全面衔接，引导高等职业院校对标高层次人才培养要求，系统优化教学体系，实现内涵式发展；同时依托本科教育资源与合作机制，助力高等职业院校加强师资建设、改善实训条件、深化教学改革，从而全面提升教育教学与人才培养质量。
在教育国际化与“职教出海”战略深入推进的背景下，本教材采用中英双语编写，旨在帮助学生夯实专业基础、提升外语应用与跨文化沟通能力，为其参与国际交流与职业发展奠定基础，同时也为“中国职业教育标准”走向国际、服务沿线国家技能人才培养提供教学资源支撑。
本书在编写过程中，深度融合产业需求与教学实际，特别感谢力鸿检验集团有限公司作为参编单位，为教材注入了行业一线的实战经验与技术标准，强化了教学内容与岗位能力的对接，充分体现了“校企合作、产教融合”的编写理念。
本书内容简明易懂，针对性和实用性较强，力求经典，且有代表性。
本书分绪论、物理化学实验基本操作、常用实验仪器使用方法、实验项目、附录五个部分。
绪论介绍了物理化学实验目的和要求、安全防护、测量误差，实验数据的表达与处理、计算机数据处理技术和实验考核要求；物理化学实验基本操作介绍了常用的温度、压力及流量等参数的测定方法；常用实验仪器使用方法着重介绍了实验中常用的仪器，如超级恒温槽、沸点测定仪、阿贝折射仪、电导率仪、电位差计、电化学工作站、旋光仪、表面张力实验装置和电泳仪等；实验项目一共9个，涵盖化学热力学、电化学、化学反应动力学、界面现象与胶体化学等方面的实验，注重学生独立思考、分析和解决问题能力的培养和训练，使学生能把学过的理论知识及实验技术加以综合运用；附录中收录了物理化学常用数据。
本书由马振雄、诸昌武和钱琛合作完成，并由刘风云教授担任主审，在此对刘风云教授的辛勤付出与严谨指导表示诚挚感谢。特别鸣谢沈发治教授，自课程建设之初便持续关注并给予大力支持，为教材的定位与架构提供了宝贵建议，对此我们深怀感激。
在本教材编写过程中，我们参考了多所兄弟院校的相关教材，汲取了其中宝贵的经验与思路。同时，特别感谢扬州大学陈铭、张恩仁、施巧芳等老师给予的悉心指导与支持，在此一并致以诚挚谢意。
由于编写时间紧、任务重，书中难免存在疏漏与不足之处，恳请广大师生和读者批评指正，以便今后完善。
编者
2025年11月
In alignment with the strategic direction for modern vocational education set forth at the 20th CPC National Congress，which emphasizes cultivating“highly skilled personnel”through vocational education and“advanced highly-skilled personnel”through vocational undergraduate programs，this bilingual textbook of physical chemistry experiment has been developed specifically for vocational undergraduate institutions and higher vocational colleges.It integrates the practical requirements of the“4+0”and“3+2”joint training models，combining practical focus with forward-looking perspective to support the systematic training of high-quality technical talent at different levels.
The vocational-undergraduate joint training initiative represents significant progress in building a modern vocational education system，playing a crucial role in enhancing teaching quality and elevating the academic standards of vocational institutions.By aligning curriculum design，teaching content，and evaluation mechanisms with undergraduate education standards，the program promotes systematic optimization of teaching systems and connotative development.Furthermore，through introducing undergraduate educational resources and collaboration mechanisms，it strengthens faculty development，improves practical training conditions，and fosters teaching innovation，thereby comprehensively elevating educational quality and talent training outcomes.
Against the backdrop of educational internationalization and the“Vocational Education Going Global”strategy，this bilingual textbook assists students in building a solid professional foundation while enhancing their foreign language application skills and cross-cultural communication competence，preparing them for international engagement and career development.It also serves as a teaching resource to support the internationalization of Chinese vocational education standards and contribute to talent development in partner countries.
The textbook deeply integrates industry needs with teaching practice.We extend sincere appreciation to Li Hong Inspection Group Co.，Ltd. for their participation in the compilation process，bringing firsthand industry experience and technical standards that effectively bridge teaching content and professional competency requirements，fully reflecting the principle of“industry-education integration and school-enterprise cooperation.”
Structured systematically and concisely，the textbook comprises five parts：Introduction，Basic Experimental Techniques，Common Instruments and Operations，Experimental Projects，and Appendices.The Introduction covers teaching objectives，assessment requirements，safety protocols，error analysis，and data processing methods.Basic Experimental Techniques focus on measuring parameters such as temperature，pressure，and flow rate.The Common Instruments section provides detailed operating guidelines for equipment including super thermostatic baths，Abbe refractometers，and conductivity meters.Nine experimental projects span chemical thermodynamics，electrochemistry，kinetics，and colloid chemistry，designed to develop students’ ability to integrate theoretical knowledge with practical problem-solving skills.
The content of this book is concise and easy to understand，with strong pertinence and practicability，and strives to be classic and representative.
This book is divided into five parts：introduction，basic experimental techniques，methods of using common experimental instruments，experimental projects，and appendices.
The introduction introduces the teaching purpose and requirements，safety protection，measurement error，experimental data expression and processing，computer data processing technology and experimental assessment requirements of physical chemistry experiments;physical chemistry basic experimental technology introduces the commonly used measurement methods of parameters such as temperature，pressure and flow;the methods of using common experimental instruments focuse on the instruments used in the experiment，such as super constant temperature bath，boiling point tester，Abbe refractometer，conductivity meter，potentiometer，electrochemical analyzer，polarimeter，surface tension test device and electrophoresis instrument，etc.; the experimental projects cover chemical thermodynamics，electrochemistry，chemical reaction kinetics，interface phenomena and colloid chemistry，etc.，a total of 9 experiments，mainly aimed at the cultivation and training of students’ independent thinking，analysis and problem-solving abilities，so that students can comprehensively apply the theoretical knowledge and experimental techniques learned; the appendix includes commonly used data in physical chemistry.
This textbook results from the collaborative efforts of Ma Zhenxiong，Zhu Changwu，and Qian Chen.We are deeply grateful to Professor Liu Fengyun for serving as chief reviewer，whose diligent work and rigorous guidance ensured the academic quality of this edition.Special thanks go to Professor Shen Fazhi for his steadfast support since the program’s inception and his valuable advice on the textbook’s positioning and structure.
We have also drawn insights from related textbooks of peer institutions and extend sincere appreciation to Chen Ming，Zhang Enren，and Shi Qiaofang of Yangzhou University for their thoughtful guidance.
Due to time constraints and the complexity of the compilation process，omissions and shortcomings are inevitable.We warmly welcome feedback from teachers and readers to inform future improvements.
The editorsNovember 2025
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